X-RAY DIFFRACTION AND MÖSSBAUER SPECTROSCOPY INVESTIGATIONS OF THE (Al, Ni, Co)-DOPED AgFeO2 SYNTHESIZED BY HYDROTHERMAL METHOD

Karolina Siedliska

doi:10.35784/iapgos.2346

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Published: Dec 20, 2020

DOI: https://doi.org/10.35784/iapgos.2346

Issue Vol. 10 No. 4 (2020)

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DOI

https://doi.org/10.35784/iapgos.2346

Authors

Karolina Siedliska

k.siedliska@pollub.pl

Lublin Univeristy of Technology, Department of Electronics and Computer Science, Poland

https://orcid.org/0000-0002-2740-8132

Abstract

Delafossite AgFeO₂, AgFe_0.9Al_0.1O₂, AgFe_0.9Ni_0.1O₂, and AgFe_0.9Co_0.1O₂ powders were synthesized by hydrothermal method. The structural analysis and hyperfine interactions investigations were performed by X-ray diffraction and the Mössbauer spectroscopy. It was found that the (Al, Ni, Co)-doped delafossite phases with traces of metallic silver can be obtained during hydrothermal synthesis. Investigations revealed that the type of the incorporated element has an impact on the structural properties of the obtained delafossites. However, doping of cobalt, nickel, and alumina ions to the AgFeO₂ delafossite structure does not cause significant changes in the values of the hyperfine interactions parameters. The of the Mössbauer spectra confirm the paramagnetic character of the obtained compounds at room temperature.

Keywords:

delafossites, hydrothermal synthesis, X-ray diffraction, Mössbauer spectroscopy

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Siedliska, K. (2020). X-RAY DIFFRACTION AND MÖSSBAUER SPECTROSCOPY INVESTIGATIONS OF THE (Al, Ni, Co)-DOPED AgFeO2 SYNTHESIZED BY HYDROTHERMAL METHOD. Informatyka, Automatyka, Pomiary W Gospodarce I Ochronie Środowiska, 10(4), 15–18. https://doi.org/10.35784/iapgos.2346

X-RAY DIFFRACTION AND MÖSSBAUER SPECTROSCOPY INVESTIGATIONS OF THE (Al, Ni, Co)-DOPED AgFeO2 SYNTHESIZED BY HYDROTHERMAL METHOD

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