Study of the zero shear viscosity of SBS copolymer modified bitumens
Mieczysław Słowik
Institute of Civil Engineering; Faculty of Civil and Environmental Engineering; Poznan University of Technology (Poland)
https://orcid.org/0000-0001-8049-591X
Marta Andrzejczak
Institute of Civil Engineering; Faculty of Civil and Environmental Engineering; Poznan University of Technology (Poland)
Abstract
The paper presents the results of the zero shear viscosity (ZSV) determined by using a dynamic shear rheometer (DSR). The tests were conducted with the use of 50/70 penetration grade bitumen produced from Venezuelan and Russian crude oils (named V50/70 and R50/70, respectively). Specimens of the tested polymer modified bitumens were combined with modified bitumen concentrate (containing 9% of SBS copolymer) by mixing them together. The objects of the tests were modified bitumens containing 1.5%; 3.0%; 4.5%; 6.0% and 9.0% of SBS copolymer. Zero shear viscosity (ZSV) was determined with the use of two methods: the creep method at various levels of shear stress in the time sequence and a method in which kinematic, sinusoidal angular deformation was applied. The tests were conducted at a constant temperature of 60˚C. The results of two ZSV tests gave similar findings for 50/70 penetration grade bitumen and modified bitumen with low SBS copolymer content (1.5%). In the case of modified bitumen with higher SBS copolymer content, i.e. 3%; 4.5%; 6%; 9%, zero shear viscosity determined by two methods gave different results.
Keywords:
zero shear viscosity (ZSV), bitumen, dynamic shear rheometer (DSR), copolymer SBS, rheological propertiesReferences
Grabowski W., Słowik M. Badania właściwości reologicznych asfaltów drogowych modyfikowanych polimerami. Foundations of Civil and Environmental Engineering (2002): 5-36.
Google Scholar
Słowik M.,Wybrane zagadnienia lepkosprężystości drogowych asfaltów modyfikowanych zawierających elastomer SBS, Rozprawy, Nr 508, Poznań, Wydawnictwo Pol. Poznańskiej 2013.
Google Scholar
Sybilski D. Polimeroasfalty drogowe, Jakość funkcjonalna, metodyka i kryteria oceny, Instytut Badawczy Dróg i Mostów, seria: Studia i materiały, zeszyt 45, Warszawa 1996.
Google Scholar
Giuliani F., Merusi F., Antunes I. Creep flow behavior of asphalt rubber. The Zero-Shear Viscosity Analysis. Proceeding of the asphalt rubber (2006).
Google Scholar
Biro Sz., Gandhi T., Amirkhanian S. Determination of zero shear viscosity of warm asphalt binder. Construction and Building Materials 23 (2009) 2080-2086.
Google Scholar
Vlachovicova Z., Wekumbura Ch., Stastna J., Zanzotto L. Creep characteristics of asphalt modified by radial styrene-butadiene-styrene copolymer. Construction and Building Materials 21 (2007) 567-577.
Google Scholar
PN-EN 14770 „Asfalty i lepiszcza asfaltowe. Oznaczenie zespolonego modułu ścinania i kąta przesunięcia fazowego w reometrze dynamicznego ścinania (DSR)” (2012).
Google Scholar
Kok B.V., Yilmaz M., Sengoz B., Sengur A., Avci E. Investigation of complex modulus of base and SBS modified bitumen with artificial neural networks, Expert Systems with Applications 37 (2010)7775-7780.
DOI: https://doi.org/10.1016/j.eswa.2010.04.063
Google Scholar
PKN-CEN/TS 15325: „Asfalty i lepiszcza asfaltowe. Oznaczenie lepkości zerowego ścinania (ZSV) metodą pełzania w reometrze dynamicznego ścinania” (2010).
Google Scholar
Authors
Mieczysław SłowikInstitute of Civil Engineering; Faculty of Civil and Environmental Engineering; Poznan University of Technology Poland
https://orcid.org/0000-0001-8049-591X
Authors
Marta AndrzejczakInstitute of Civil Engineering; Faculty of Civil and Environmental Engineering; Poznan University of Technology Poland
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